2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile

Base Information

Chemical Name:2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile
CAS No.:258500-77-5
Molecular Formula:C₁₆H₂₁Cl₂NO₄
Molecular Weight:362.253
Hs Code.:

Synonyms:2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile

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Chemical Property of 2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile

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Technology Process of 2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile

There total 1 articles about 2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 7252-83-7
1-bromo-2,2-dimethoxyethane

: 3218-49-3
3,4-dichloro-benzeneacetonitrile

: 258500-77-5
2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile

Guidance literature:: With sodium amide; In toluene; Heating;
DOI:10.1021/jm0401614

Reference yield: 56.0%

: 100-46-9
benzylamine

: 258500-77-5
2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile

: 1-benzyl-4-(3,4-dichlorophenyl)-piperidine-4-carbonitrile

Guidance literature:: 2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile; With hydrogenchloride; at 50 ℃;

benzylamine; With sodium cyanoborohydride; In methanol; for 48h;
DOI:10.1016/j.bmc.2005.05.025

Reference yield: 36.0%

: 30684-05-0
3-phenylpropylamine hydrochloride

: 258500-77-5
2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile

: 4-(3,4-dichlorophenyl)-1-(3-phenylpropyl)-piperidine-4-carbonitrile

Guidance literature:: 2-(3,4-dichlorophenyl)-2-(2,2-dimethoxyethyl)-4,4-dimethoxybutyronitrile; With hydrogenchloride; at 50 ℃;

3-phenylpropylamine hydrochloride; With sodium cyanoborohydride; In methanol; for 48h;
DOI:10.1016/j.bmc.2005.05.025