C₂₆H₂₃N₃O₅

Base Information

Chemical Name:C₂₆H₂₃N₃O₅
CAS No.:1380110-12-2
Molecular Formula:C₂₆H₂₃N₃O₅
Molecular Weight:457.486
Hs Code.:

C<sub>26</sub>H<sub>23</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₆H₂₃N₃O₅

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Chemical Property of C₂₆H₂₃N₃O₅

Chemical Property:

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Technology Process of C₂₆H₂₃N₃O₅

There total 6 articles about C₂₆H₂₃N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1380110-10-0
C₂₆H₂₃N₃O₄

: 1380110-12-2
C₂₆H₂₃N₃O₅

Guidance literature:: C₂₆H₂₃N₃O₄; With urea hydrogen peroxide adduct; trifluoroacetic anhydride; In acetonitrile; at 0 - 25 ℃; for 17h;

With sodium hydrogencarbonate; In water; ethyl acetate; acetonitrile;

Reference yield:

: 112334-42-6
benzyl 4,5-bis(benzyloxy)picolinate

: 1380110-12-2
C₂₆H₂₃N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

1.2: -78 - 25 °C

2.1: hydroxylamine hydrochloride; sodium hydrogencarbonate; sodium sulfate / acetonitrile / 0.17 h / 150 °C / Microwave irradiation

2.2: 0.25 h / 170 °C / Microwave irradiation

3.1: sodium methylate / methanol / 17 h / 20 - 25 °C

3.2: 25.5 h

4.1: 1,4-dioxane / 9.5 h / Reflux

5.1: urea hydrogen peroxide adduct; trifluoroacetic anhydride / acetonitrile / 17 h / 0 - 25 °C

With hydroxylamine hydrochloride; sodium methylate; urea hydrogen peroxide adduct; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium sulfate; trifluoroacetic anhydride; In 1,4-dioxane; methanol; dichloromethane; toluene; acetonitrile;

Reference yield:

: 4,5-bis(benzyloxy)picolinaldehyde

: 1380110-12-2
C₂₆H₂₃N₃O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; sodium hydrogencarbonate; sodium sulfate / acetonitrile / 0.17 h / 150 °C / Microwave irradiation

1.2: 0.25 h / 170 °C / Microwave irradiation

2.1: sodium methylate / methanol / 17 h / 20 - 25 °C

2.2: 25.5 h

3.1: 1,4-dioxane / 9.5 h / Reflux

4.1: urea hydrogen peroxide adduct; trifluoroacetic anhydride / acetonitrile / 17 h / 0 - 25 °C

With hydroxylamine hydrochloride; sodium methylate; urea hydrogen peroxide adduct; sodium hydrogencarbonate; sodium sulfate; trifluoroacetic anhydride; In 1,4-dioxane; methanol; acetonitrile;