(methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one

Base Information

Chemical Name:(methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one
CAS No.:126412-20-2
Molecular Formula:C₁₇H₂₀O₃S₂
Molecular Weight:336.476
Hs Code.:

Synonyms:(methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one

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Chemical Property of (methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one

Chemical Property:

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Technology Process of (methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one

There total 3 articles about (methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3866-79-3
1,3-bis(p-toluenesulfonylthio)propane

: 126412-19-9
(methoxymethylenoxy-2' phenyl)-3 formyl-6 cyclohexen-2 one

: 126412-20-2
(methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one

Guidance literature:: With potassium acetate; In ethanol; for 24h; Heating;
DOI:10.1016/0223-5234(89)90082-2

Reference yield:

: 68314-54-5
1-bromo-2-(methoxymethoxy)benzene

: 126412-20-2
(methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / Mg / tetrahydrofuran; 1,2-dibromo-ethane / 2 h / Heating

2: 80 percent / NaH / tetrahydrofuran / 2 h

3: 80 percent / KOAc / ethanol / 24 h / Heating

With potassium acetate; sodium hydride; magnesium; In tetrahydrofuran; ethanol; ethylene dibromide;
DOI:10.1016/0223-5234(89)90082-2

Reference yield:

: 79237-23-3
(methoxymethylenoxy-2' phenyl)-3 cyclohexen-2 one

: 126412-20-2
(methoxymethylenoxy-2' phenyl)-3 (dithio-1,3 propyl)-6 cyclohexen-2 one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaH / tetrahydrofuran / 2 h

2: 80 percent / KOAc / ethanol / 24 h / Heating

With potassium acetate; sodium hydride; In tetrahydrofuran; ethanol;
DOI:10.1016/0223-5234(89)90082-2