2,5-dichloro-4-[hydroxy-(5-methoxymethoxy-benzo-[1,3]dioxol-4-yl)-methyl]-3,6-diisopropoxybenzoic acid methyl ester

Base Information

Chemical Name:2,5-dichloro-4-[hydroxy-(5-methoxymethoxy-benzo-[1,3]dioxol-4-yl)-methyl]-3,6-diisopropoxybenzoic acid methyl ester
CAS No.:1065246-71-0
Molecular Formula:C₂₄H₂₈Cl₂O₉
Molecular Weight:531.387
Hs Code.:

Synonyms:2,5-dichloro-4-[hydroxy-(5-methoxymethoxy-benzo-[1,3]dioxol-4-yl)-methyl]-3,6-diisopropoxybenzoic acid methyl ester

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Chemical Property of 2,5-dichloro-4-[hydroxy-(5-methoxymethoxy-benzo-[1,3]dioxol-4-yl)-methyl]-3,6-diisopropoxybenzoic acid methyl ester

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Technology Process of 2,5-dichloro-4-[hydroxy-(5-methoxymethoxy-benzo-[1,3]dioxol-4-yl)-methyl]-3,6-diisopropoxybenzoic acid methyl ester

There total 1 articles about 2,5-dichloro-4-[hydroxy-(5-methoxymethoxy-benzo-[1,3]dioxol-4-yl)-methyl]-3,6-diisopropoxybenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1065246-70-9
2,5-dichloro-4-formyl-3,6-diisopropoxybenzoic acid methyl ester

: 111726-43-3
3,4-(methylenedioxy)phenyl methoxymethyl ether

: 1065246-71-0
2,5-dichloro-4-[hydroxy-(5-methoxymethoxy-benzo-[1,3]dioxol-4-yl)-methyl]-3,6-diisopropoxybenzoic acid methyl ester

Guidance literature:: 3,4-(methylenedioxy)phenyl methoxymethyl ether; With n-butyllithium; In hexane; toluene; at 0 ℃; for 1h; Inert atmosphere;

2,5-dichloro-4-formyl-3,6-diisopropoxybenzoic acid methyl ester; In tetrahydrofuran; hexane; toluene; at -78 - -20 ℃; Inert atmosphere;
DOI:10.1021/ol801962a