(R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate

Base Information

Chemical Name:(R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate
CAS No.:131557-00-1
Molecular Formula:C₂₂H₃₈O₅Si
Molecular Weight:410.626
Hs Code.:

Synonyms:(R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate

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Chemical Property of (R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate

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Technology Process of (R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate

There total 1 articles about (R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 131556-98-4,131557-15-8
(RS)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol

: 108-24-7
acetic anhydride

: 131557-00-1
(R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate

Guidance literature:: With pyridine; Ambient temperature;

Reference yield:

: 131557-00-1
(R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate

: 133709-52-1
(R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxohexahydroindan-7-yl>-4-<<(4-methylphenyl)sulfonyl>oxy>butane-1-ol acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 50percent HF / acetonitrile / Ambient temperature

2: pyridine / Ambient temperature

With pyridine; hydrogen fluoride; In acetonitrile;

Reference yield:

: 131557-00-1
(R)-1-<(3aR,7S,7aR)-3a-methyl-3,6-dioxo-hexahydroindan-7-yl>-4-<(1,1-dimethylethyl)dimethylsilyloxy>butan-1-ol acetate

: C₃₄H₃₈IO₄P

Guidance literature:: Multi-step reaction with 4 steps

1: 50percent HF / acetonitrile / Ambient temperature

2: pyridine / Ambient temperature

3: NaI / acetone / Heating

4: acetonitrile / Heating

With pyridine; hydrogen fluoride; sodium iodide; In acetone; acetonitrile;