β-phenyl-2-carboxycinnamic acid

Base Information

Chemical Name:β-phenyl-2-carboxycinnamic acid
CAS No.:101278-30-2
Molecular Formula:C₁₆H₁₂O₄
Molecular Weight:268.269
Hs Code.:

Synonyms:β-phenyl-2-carboxycinnamic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-phenyl-2-carboxycinnamic acid

Chemical Property:

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Technology Process of β-phenyl-2-carboxycinnamic acid

There total 6 articles about β-phenyl-2-carboxycinnamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 36159-76-9
4-phenyl-1-naphthol

: 101278-30-2
β-phenyl-2-carboxycinnamic acid

Guidance literature:: With oxone; In water; acetonitrile; at 20 ℃; for 13h;
DOI:10.1021/acs.joc.5b00292

Reference yield:

: 2-(2-tert-butoxycarbonyl-1-phenyl-vinyl)-benzoic acid

: 101278-30-2
β-phenyl-2-carboxycinnamic acid

Guidance literature:: With toluene-4-sulfonic acid;
DOI:10.1021/ja01157a133

Reference yield:

: 85-52-9
2-Benzoylbenzoic acid

: 101278-30-2
β-phenyl-2-carboxycinnamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: concentrated H₂SO₄

2: NaH; tert-butyl alcohol

3: toluene-4-sulfonic acid

With sulfuric acid; sodium hydride; toluene-4-sulfonic acid; tert-butyl alcohol;
DOI:10.1021/ja01157a133