2-CARBOETHOXYBENZOPHENONE

Base Information

• Chemical Name: 2-CARBOETHOXYBENZOPHENONE
• CAS No.: 604-61-5
• Molecular Formula: C16H14 O3
• Molecular Weight: 254.285
• Hs Code.: 2914509090
• Mol file: 604-61-5.mol

Synonyms:Benzoicacid, o-benzoyl-, ethyl ester (7CI,8CI); 2-Carbethoxybenzophenone; Ethyl2-benzoylbenzoate; Ethyl o-benzoylbenzoate; Ketonone E; NSC 6804

Chemical Property of 2-CARBOETHOXYBENZOPHENONE

Chemical Property:

• Vapor Pressure: 1.56E-05mmHg at 25°C
• Melting Point: 59.5°C
• Refractive Index: 1.5600 (estimate)
• Boiling Point: 365.6°C at 760 mmHg
• Flash Point: 160.3°C
• PSA: 43.37000
• Density: 1.145g/cm³
• LogP: 3.09430

Purity/Quality:

≥97.0% ^*data from raw suppliers

2-carboethoxybenzophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Plasticizer for nitrocellulose and synthetic resins.

Technology Process of 2-CARBOETHOXYBENZOPHENONE

There total 15 articles about 2-CARBOETHOXYBENZOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-Benzoylbenzoic acid (85-52-9) + ethyl iodide (75-03-6) → ethyl 2-benzoylbenzoate (604-61-5)

Guidance literature:

With cesium fluoride; In N,N-dimethyl-formamide; at 10 - 15 ℃; for 24h;

DOI:10.1021/jo00033a048

Reference yield: 89.0%

benzoyl chloride (98-88-4) + (2-(ethoxycarbonyl)phenyl)zinc(II) bromide → ethyl 2-benzoylbenzoate (604-61-5)

Guidance literature:

With bis(acetylacetonate)nickel(II); In tetrahydrofuran; at 20 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2011.01.135

Reference yield: 80.0%

2-Benzoylbenzoic acid (85-52-9) + ethanol (64-17-5) → ethyl 2-benzoylbenzoate (604-61-5)

Guidance literature:

With sulfuric acid; for 0.666667h; Reflux;

DOI:10.1007/s00044-012-0270-0

upstream raw materials:

2-Benzoylbenzoic acid

ethanol

2-benzoylbenzoyl chloride

methyl o-benzoylbenzoate

Downstream raw materials:

3-methyl-3-phenylphthalide

2-(1-phenylethenyl)benzoic acid

2-Benzylbenzoic acid

2-benzyltoluene

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