1,2-diethoxy-1,2-dimethyldiphenyldisilane

Base Information

Chemical Name:1,2-diethoxy-1,2-dimethyldiphenyldisilane
CAS No.:142684-21-7
Molecular Formula:C₁₈H₂₆O₂Si₂
Molecular Weight:330.574
Hs Code.:

Synonyms:1,2-diethoxy-1,2-dimethyldiphenyldisilane

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Chemical Property of 1,2-diethoxy-1,2-dimethyldiphenyldisilane

Chemical Property:

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Technology Process of 1,2-diethoxy-1,2-dimethyldiphenyldisilane

There total 1 articles about 1,2-diethoxy-1,2-dimethyldiphenyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: 766-08-5,146088-00-8
methylphenylsilane

: 4313-76-2
1,3-Diaethoxy-1,3-dimethyl-1,3-diphenyl-disiloxan

: 142684-20-6
C₁₆H₂₂OSi₂

: 142684-21-7
1,2-diethoxy-1,2-dimethyldiphenyldisilane

: 142684-22-8
C₂₃H₃₀OSi₃

Guidance literature:: With norborn-2-ene; bis(cyclopentadienyl)titanium dichloride; n-butyllithium; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) THF, hexane, reflux, 100min, 2.) THF, hexane, RT;
DOI:10.1016/0022-328X(92)83095-Y

Reference yield: 57.0%

: 142684-21-7
1,2-diethoxy-1,2-dimethyldiphenyldisilane

: 536-74-3
phenylacetylene

: 161991-66-8
(Z)-1,2-bis(ethoxymethylphenylsilyl)phenylethene

Guidance literature:: With palladium diacetate; tert-butylisonitrile; In toluene; at 70 ℃; for 5h;
DOI:10.1016/0022-328X(94)05151-Z

Reference yield:

: 142684-21-7
1,2-diethoxy-1,2-dimethyldiphenyldisilane

: 1,3-dimethyl-1,3,4-triphenyl-2-oxa-1,3-disilacyclopent-4-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / Pd(OAc)2, tert-butylisonitrile / toluene / 5 h / 70 °C

2: 82 percent / acetyl chloride / 10 h / 50 °C

3: 81 percent / H₂O / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature

With palladium diacetate; tert-butylisonitrile; water; acetyl chloride; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1016/0022-328X(94)05151-Z