3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

Base Information

Chemical Name:3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol
CAS No.:81535-88-8
Molecular Formula:C₃₉H₃₁BrO₄
Molecular Weight:643.577
Hs Code.:

Synonyms:3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

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Chemical Property of 3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

Chemical Property:

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Technology Process of 3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

There total 6 articles about 3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 81535-87-7
2-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-4-phenylphenol

: 81535-88-8
3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

Guidance literature:: With potassium hydroxide; In water; for 144h; Ambient temperature;
DOI:10.1021/jo00135a005

Reference yield:

: 92-69-3
4-Phenylphenol

: 81535-88-8
3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / bromine / CHCl₃ / 60 °C

2: 49 percent / KOH / H₂O / 72 h / 40 °C

3: 71 percent / conc. HCl / xylene / 20 h / Heating

4: 48 percent / KOH / H₂O / 144 h / 35 °C

5: 65 percent / conc. HCl / xylene / 20 h / Heating

6: 73 percent / KOH / H₂O / 144 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; bromine; In chloroform; water; xylene;
DOI:10.1021/jo00135a005

Reference yield:

: 92-03-5
2-bromo-4-phenylphenol

: 81535-88-8
3-<3-(3-bromo-5-phenylsalicyl)-5-phenylsalicyl>-5-phenyl-2-hydroxybenzyl alcohol

Guidance literature:: Multi-step reaction with 5 steps

1: 49 percent / KOH / H₂O / 72 h / 40 °C

2: 71 percent / conc. HCl / xylene / 20 h / Heating

3: 48 percent / KOH / H₂O / 144 h / 35 °C

4: 65 percent / conc. HCl / xylene / 20 h / Heating

5: 73 percent / KOH / H₂O / 144 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; In water; xylene;
DOI:10.1021/jo00135a005