6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine

Base Information

Chemical Name:6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine
CAS No.:1438406-50-8
Molecular Formula:C₂₂H₂₈N₂O₃S₂
Molecular Weight:432.608
Hs Code.:

Synonyms:6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine

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Chemical Property of 6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine

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Technology Process of 6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine

There total 9 articles about 6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.8%

: 1438406-50-8
6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine

Guidance literature:: With pyridine; at 25 - 30 ℃; Inert atmosphere;

Reference yield:

: 1438407-72-7
C₁₆H₂₄N₂OS

: 98-09-9
benzenesulfonyl chloride

: 1438406-50-8
6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine

Guidance literature:: With pyridine; at 25 - 30 ℃; Inert atmosphere;

Reference yield:

: 1438407-69-2
(6-hydroxy-2H-benzo[b][1,4]thiazin-4(3H)-yl)(phenyl)methanone

: 1438406-50-8
6-(3-(2-methylpyrrolidin-1-yl)propoxy)-4-(phenylsulfonyl)-3,4-dihydro-2H-benzo[b][1,4]thiazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 25 °C / Inert atmosphere

1.2: 75 - 80 °C

2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 0.5 h / Inert atmosphere

2.2: 75 - 80 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 30 °C / Inert atmosphere

4.1: pyridine / 25 - 30 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; potassium carbonate; potassium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;