3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid

Base Information

Chemical Name:3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid
CAS No.:1449664-50-9
Molecular Formula:C₁₆H₁₆N₄O₂
Molecular Weight:296.329
Hs Code.:

Synonyms:3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid

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Chemical Property of 3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid

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Technology Process of 3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid

There total 3 articles about 3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 607373-83-1
2-chloro-4-methoxy-5-nitro-pyridine

: 1449664-50-9
3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid

: 1449664-49-6
N-(2-methoxyethyl)-3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethanol / 0.25 h / 150 °C / Microwave irradiation

2.1: dmap / acetonitrile / 16 h / 20 °C

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 48 h / 20 °C / 760.05 Torr

4.1: 1 h / 100 °C

5.1: hydrogenchloride / 1,4-dioxane; methanol / 72 h / 20 °C

6.1: dibenzylideneacetone bis(triphenylphiosphine) palladium⁽⁰⁾; sodium t-butanolate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 90 °C

7.1: trimethylaluminum / chloroform / 0.33 h / 20 °C / Inert atmosphere

7.2: 24 h / 50 °C

With hydrogenchloride; dmap; dibenzylideneacetone bis(triphenylphiosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; trimethylaluminum; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; In 1,4-dioxane; methanol; ethanol; chloroform; acetonitrile;

Reference yield:

: 1449664-38-3
methyl 3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzoate

: 109-85-3
2-methoxyethylamine

: 1449664-50-9
3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid

: 1449664-49-6
N-(2-methoxyethyl)-3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzamide

Guidance literature:: 2-methoxyethylamine; With trimethylaluminum; In chloroform; at 20 ℃; for 0.333333h; Inert atmosphere;

methyl 3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzoate; In chloroform; at 50 ℃; for 24h;

Reference yield:

: 1449668-91-0
N,1-dimethyl-1H-imidazo[4,5-c]pyridin-6-amine

: 1449664-50-9
3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzic acid

: 1449664-49-6
N-(2-methoxyethyl)-3-methyl-4-(methyl(1-methyl-1H-imidazo[4,5-c]pyridin-6-yl)amino)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dibenzylideneacetone bis(triphenylphiosphine) palladium⁽⁰⁾; sodium t-butanolate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 90 °C

2.1: trimethylaluminum / chloroform / 0.33 h / 20 °C / Inert atmosphere

2.2: 24 h / 50 °C

With dibenzylideneacetone bis(triphenylphiosphine) palladium⁽⁰⁾; trimethylaluminum; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; In 1,4-dioxane; chloroform;