2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol

Base Information

Chemical Name:2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol
CAS No.:89827-38-3
Molecular Formula:C₃₄H₂₈O₃
Molecular Weight:484.595
Hs Code.:

2-(2,10-dimethyl-6,6-diphenyldibenzo<d,f><1,3>dioxepin-4-yl)-4-methylphenol

Synonyms:2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol

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Technology Process of 2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol

There total 1 articles about 2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2051-90-3
Dichlorodiphenylmethane

: 71128-89-7
2,2',2''-trihydroxy-5,5',5''-trimethyl-m-terphenyl

: 89827-38-3
2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol

Guidance literature:: at 180 - 190 ℃; for 0.583333h;
DOI:10.1021/ja00323a037

Reference yield: 100.0%

: 100-39-0
benzyl bromide

: 89827-38-3
2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol

: 89827-39-4
2,10-dimethyl-4-<5-methyl-2-(phenylmethoxy)phenyl>-6,6-diphenyldibenzo<1,3>dioxepin

Guidance literature:: With potassium carbonate; In acetone; for 78h; Heating; in dark;
DOI:10.1021/ja00323a037

Reference yield:

: 89827-38-3
2-(2,10-dimethyl-6,6-diphenyldibenzo<1,3>dioxepin-4-yl)-4-methylphenol

: 89827-44-1
2',2'',2''',2''''-tetramethoxy-5,5',5'',5''',5'''',5'''''-hexamethyl-<1,1':3',1'':3'',1''':3''',1'''':3'''',1'''''-sexiphenyl>2,2'''''-diol

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / K₂CO₃ / acetone / 78 h / Heating; in dark

2: 97 percent / glacial acetic acid / H₂O / 30 h / Heating

3: 93 percent / 2,4,4,6-tetrabromocyclohexa-2,5-dienone / CHCl₃ / 4 h / 0 °C

4: NaOH / tetrahydrofuran; H₂O / 1.5 h / Heating

5: 1.) BuLi; 2.) Fe(acac)3 / 1.) THF, hexane, -78 deg C, 10 min; 2.) benzene, reflux, 2.5 h

6: 97 percent / H₂ / Pd/C / ethanol; ethyl acetate / 1 h / 25 °C / 1900 Torr

With sodium hydroxide; n-butyllithium; iron(III)-acetylacetonate; 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; chloroform; water; ethyl acetate; acetone;
DOI:10.1021/ja00323a037