3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)

Base Information

Chemical Name:3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)
CAS No.:120622-47-1
Molecular Formula:C₃₈H₃₈N₄O₈
Molecular Weight:678.742
Hs Code.:

Synonyms:3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)

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Chemical Property of 3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)

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Technology Process of 3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)

There total 4 articles about 3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 112-26-5,27252-69-3
1,2-bis(2-chloroethoxy)ethane

: 120075-51-6
5-(benzyloxy)-6-methoxyquinazolin-4(3H)-one

: 120622-47-1
3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 50 ℃; for 15h;
DOI:10.1248/cpb.36.3933

Reference yield:

: 2426-61-1
2-(benzyloxy)-3-methoxy-6-nitrobenzaldehyde

: 120622-47-1
3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / 10percent aq. potassium permanganate / acetone / 7 h / 40 °C

2: 79 percent / FeSO₄*7H₂O, 8M NH₄OH / H₂O / 0.5 h / Heating

3: 80 percent / piperidine / ethanol / 30 h / Heating

4: 57 percent / sodium hydride / dimethylformamide / 15 h / 50 °C

With piperidine; ammonium hydroxide; potassium permanganate; sodium hydride; iron(II) sulfate; In ethanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1248/cpb.36.3933

Reference yield:

: 120075-49-2
6-amino-2-benzyloxy-3-methoxybenzoic acid

: 120622-47-1
3,3'-(3,6-dioxaoctamethylene)bis(5-benzyloxy-6-methoxy-4(3H)-quinazolinone)

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / piperidine / ethanol / 30 h / Heating

2: 57 percent / sodium hydride / dimethylformamide / 15 h / 50 °C

With piperidine; sodium hydride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3933