Methyl alpha-ethenyl-4-ethoxybenzeneacetate

Base Information

Chemical Name:Methyl alpha-ethenyl-4-ethoxybenzeneacetate
CAS No.:80768-39-4
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:
DSSTox Substance ID:DTXSID301281224

Synonyms:Methyl alpha-ethenyl-4-ethoxybenzeneacetate;DTXSID301281224;80768-39-4

Suppliers and Price of Methyl alpha-ethenyl-4-ethoxybenzeneacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl alpha-ethenyl-4-ethoxybenzeneacetate

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:220.109944368
Heavy Atom Count:16
Complexity:229

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC1=CC=C(C=C1)C(C=C)C(=O)OC

Technology Process of Methyl alpha-ethenyl-4-ethoxybenzeneacetate

There total 3 articles about Methyl alpha-ethenyl-4-ethoxybenzeneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80768-37-2,80768-38-3
(Z)-2-(4-Ethoxy-phenyl)-but-2-enoic acid methyl ester

: 80768-39-4
methyl 2-(4-ethoxyphenyl)but-3-enoate

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

Reference yield:

: 80768-36-1
methyl 4-ethoxyphenylglyoxylate

: 80768-39-4
methyl 2-(4-ethoxyphenyl)but-3-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, RT, 0.5 h, 2.) RT, 1 h

2: LDA / tetrahydrofuran; hexane / 2 h / -78 °C

With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane;

Reference yield:

: 103-73-1
Phenetole

: 80768-39-4
methyl 2-(4-ethoxyphenyl)but-3-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) AlCl₃ / 1.) CHCl₃, 5 deg C, 40 min, 2.) 20 deg C, 2.5 h

2: 1.) n-BuLi / 1.) THF, hexane, RT, 0.5 h, 2.) RT, 1 h

3: LDA / tetrahydrofuran; hexane / 2 h / -78 °C

With n-butyllithium; aluminium trichloride; lithium diisopropyl amide; In tetrahydrofuran; hexane;