2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane

Base Information

Chemical Name:2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane
CAS No.:76455-61-3
Molecular Formula:C₂₅H₁₈Cl₄O₆
Molecular Weight:556.226
Hs Code.:

Synonyms:2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane

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Technology Process of 2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane

There total 1 articles about 2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 2435-53-2
o-tetrachloroquinone

: 32652-95-2
O-acetylvanillal-p-methylacetophenone

: 76455-61-3
2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane

Guidance literature:: In benzene; for 20h; Heating;

Reference yield: 80.0%

: 76455-61-3
2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane

: 76455-63-5
[5,6,7,8-Tetrachloro-3-(4-hydroxy-3-methoxy-phenyl)-2,3-dihydro-benzo[1,4]dioxin-2-yl]-p-tolyl-methanone oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; for 3h; Heating;

Reference yield:

: 76455-61-3
2-(4'-acetyl-3'-methoxyphenyl)-3-(p-tolyl)-5,6,7,8-tetrachlorobenzo-p-dioxane

: 76455-64-6
C₂₇H₂₃Cl₄N₃O₇

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / hydroxylamine hydrochloride, pyridine / ethanol / 3 h / Heating

2: 60 percent

With pyridine; hydroxylamine hydrochloride; In ethanol;