6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide

Base Information

Chemical Name:6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide
CAS No.:1610021-63-0
Molecular Formula:C₂₂H₂₅N₅O₂S
Molecular Weight:423.539
Hs Code.:

Synonyms:6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide

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Chemical Property of 6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide

Chemical Property:

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Technology Process of 6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide

There total 5 articles about 6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1447226-51-8
6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)nicotinic acid

: 675112-40-0
4-aminocyclohexan-1-one hydrochloride

: 1610021-63-0
6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 1011464-52-0
6-chloro-4-isopropylamino-nicotinic acid ethyl ester

: 1610021-63-0
6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane; water / 12 h / 115 °C

2: water; lithium hydroxide / ethanol / 12 h / 20 °C

3: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; sodium carbonate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium hydroxide; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1447226-49-4
ethyl 6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)nicotinate

: 1610021-63-0
6-(benzo[d]thiazol-6-ylamino)-4-(isopropylamino)-N-(4-oxocyclohexyl)nicotinamide

Guidance literature:: Multi-step reaction with 2 steps

1: water; lithium hydroxide / ethanol / 12 h / 20 °C

2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In ethanol; N,N-dimethyl-formamide;