(S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

Base Information

Chemical Name:(S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid
CAS No.:1429753-17-2
Molecular Formula:C₁₆H₂₄N₂O₅Se
Molecular Weight:403.337
Hs Code.:

Synonyms:(S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

Suppliers and Price of (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

There total 5 articles about (S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1429753-16-1
(S)-tert-butyl (1-oxo-3-phenyl-1-((2-selenocyanatoethyl)amino)propan-2-yl)carbamate

: 1429753-17-2
(S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

Guidance literature:: With 3,3-dimethyldioxirane; In dichloromethane;
DOI:10.3390/molecules18021963

Reference yield: 63.0%

: 1429753-18-3
(S)-Se-(2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethyl) 2-phenylethaneselenoate

: 1429753-17-2
(S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

Guidance literature:: With 3,3-dimethyldioxirane; In dichloromethane;
DOI:10.3390/molecules18021963

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1429753-17-2
(S)-2-(2-((tert-butoxycarbonyl)amino)-3-phenylpropanamido)ethaneseleninic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / acetonitrile / 0.25 h / 0 °C

1.2: 12 h / 0 - 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.25 h / -50 °C

2.2: 2 h / -50 - 23 °C

3.1: 3,3-dimethyldioxirane / dichloromethane

With di-isopropyl azodicarboxylate; 3,3-dimethyldioxirane; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.3390/molecules18021963