Technology Process of C33H39NO6
There total 4 articles about C33H39NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
N,N-dimethyl-formamide;
at 60 ℃;
for 8h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2012.05.124
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride / water; toluene / Reflux
2: sodium cyanoborohydride / ethanol / 20 °C / Cooling with ice
3: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Cooling with ice
4: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere
With
hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium(0); sodium cyanoborohydride; sodium carbonate; triethylamine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
4: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.05.124
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium cyanoborohydride / ethanol / 20 °C / Cooling with ice
2: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Cooling with ice
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C / Inert atmosphere
With
dmap; tetrakis(triphenylphosphine) palladium(0); sodium cyanoborohydride; sodium carbonate; triethylamine;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
3: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.05.124
