tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate

Base Information

Chemical Name:tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate
CAS No.:1182206-87-6
Molecular Formula:C₁₉H₂₃N₃O₆
Molecular Weight:389.408
Hs Code.:

tert-butyl N<sub>4</sub>-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate

Synonyms:tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate

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Chemical Property of tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate

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Technology Process of tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate

There total 1 articles about tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1-(tert-butoxycarbonylmethyl)-4-N-(benzyloxycarbonyl)cytosine

: 1182206-87-6
tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate

Guidance literature:: N,N-dimethyl-formamide; 1-(tert-butoxycarbonylmethyl)-4-N-(benzyloxycarbonyl)cytosine; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -72 - 0 ℃; Inert atmosphere;

With acetic acid; In tetrahydrofuran; hexane; at 20 ℃; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; hexane; Inert atmosphere;
DOI:10.1002/hlca.200900047

Reference yield:

: 1182206-87-6
tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate

: 1182206-88-7
C₁₉H₂₂BrN₃O₅

Guidance literature:: tert-butyl N₄-[(benzyloxy)carbonyl]-6-(hydroxymethyl)cytosine-1-acetate; With N-ethyl-N,N-diisopropylamine; Methanesulfonic anhydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With lithium bromide; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/hlca.200900047