3-amino-4-phenylfuroxane

Base Information

• Chemical Name: 3-amino-4-phenylfuroxane
• CAS No.: 29945-54-8
• Molecular Formula: C₈H₇N₃O₂
• Molecular Weight: 177.162
• Mol file: 29945-54-8.mol

Synonyms:3-amino-4-phenylfuroxane

Chemical Property of 3-amino-4-phenylfuroxane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3-amino-4-phenylfuroxane

There total 8 articles about 3-amino-4-phenylfuroxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3-(N-nitroamino)-4-phenylfuroxan (1415839-39-2) → 3-amino-4-phenylfuroxane (29945-54-8) + 3-[(E)-(methoxy-ONN-azoxy)-4-phenyl]-1,2,5-oxadiazole-2-oxide (1415839-40-5) + 3-(N-methyl-N-nitro)amino-4-phenyl-1,2,5-oxadiazole-2-oxide (1415839-41-6)

Guidance literature:

In diethyl ether; at 0 - 5 ℃;

DOI:10.1007/s11172-012-0048-z

Reference yield:

phenylglyoxal-(1Z,2E)-dioxime (26527-40-2) → 3-amino-4-phenylfuroxane (29945-54-8)

Guidance literature:

With ammonium hydroxide; potassium hexacyanoferrate(III);

DOI:10.1002/hlca.19700530738

Reference yield:

N-hydroxy-2-(Z)-hydroxyimino-2-phenyl-acetamidine (29939-70-6) → 3-amino-4-phenylfuroxane (29945-54-8)

Guidance literature:

With hydrogenchloride; bromine; at 0 - 5 ℃;

DOI:10.1002/hlca.19700530738

upstream raw materials:

phenylglyoxal-(1Z,2E)-dioxime

N-hydroxy-2-(Z)-hydroxyimino-2-phenyl-acetamidine

3-phenyl-furazan 5-oxide

(Z)-2-(hydroxyimino)-2-phenylacetonitrile

Downstream raw materials:

4-phenyl-furazan-3-ylamine

4-amino-3-phenylfuroxane

3-phenyl-furazan 2-oxide

3-nitro-4-phenyl-1,2,5-oxadiazole 2-oxide