N-(2-bromophenyl)-3-methylbenzamide

Base Information

• Chemical Name: N-(2-bromophenyl)-3-methylbenzamide
• CAS No.: 331719-47-2
• Molecular Formula: C₁₄H₁₂BrNO
• Molecular Weight: 290.159
• Mol file: 331719-47-2.mol

Synonyms:N-(2-bromophenyl)-3-methylbenzamide

Chemical Property of N-(2-bromophenyl)-3-methylbenzamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

N-(2-BROMOPHENYL)-3-METHYLBENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2-bromophenyl)-3-methylbenzamide

There total 1 articles about N-(2-bromophenyl)-3-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromoaniline (615-36-1) + 3-Methylbenzoyl chloride (1711-06-4) → N-(2-bromophenyl)-3-methylbenzamide (331719-47-2)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1016/j.bmc.2010.02.057

Reference yield: 97.0%

N-(2-bromophenyl)-3-methylbenzamide (331719-47-2) → 2-(3-methylphenyl)benzoxazole (14625-58-2)

Guidance literature:

With copper(II) ferrite; potassium carbonate; In dimethyl sulfoxide; at 120 ℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube;

DOI:10.1055/s-0033-1340599

Reference yield: 86.0%

N-(2-bromophenyl)-3-methylbenzamide (331719-47-2) → N-(2-bromophenyl)-3-methylbenzothioamide

Guidance literature:

With Lawessons reagent; In toluene; for 2h; Reflux; Inert atmosphere;

DOI:10.1021/acs.orglett.1c00235

upstream raw materials:

2-bromoaniline

3-Methylbenzoyl chloride

Downstream raw materials:

2-(3-methylphenyl)benzoxazole