S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

Base Information

Chemical Name:S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate
CAS No.:1403889-62-2
Molecular Formula:C₁₃H₁₄FNO₄S₂
Molecular Weight:331.389
Hs Code.:

Synonyms:S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

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Chemical Property of S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

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Technology Process of S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

There total 4 articles about S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: N-acetoxy-N-(2-fluorophenyl)-2-chloroacetamide

: 140-89-6
potassium ethyl xanthogenate

: 1403889-62-2
S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

Guidance literature:: In acetone; for 6h; Inert atmosphere;
DOI:10.1021/ol3026044

Reference yield:

: 1403889-51-9
C₈H₇ClFNO₂

: 1403889-62-2
S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride / 20 °C / Inert atmosphere

2: acetone / 6 h / Inert atmosphere

With acetic anhydride; In acetone;
DOI:10.1021/ol3026044

Reference yield:

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 1403889-62-2
S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium chloride; zinc / ethanol; water / 4 h / 10 °C / Cooling with ice; Inert atmosphere

2: sodium hydrogencarbonate / diethyl ether; water / -5 °C / Cooling with ice; Inert atmosphere

3: acetic anhydride / 20 °C / Inert atmosphere

4: acetone / 6 h / Inert atmosphere

With acetic anhydride; sodium hydrogencarbonate; ammonium chloride; zinc; In diethyl ether; ethanol; water; acetone;
DOI:10.1021/ol3026044