S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate

Base Information

Chemical Name:S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate
CAS No.:1403889-71-3
Molecular Formula:C₂₂H₃₁BFNO₆S₂
Molecular Weight:499.433
Hs Code.:

Synonyms:S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate

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Chemical Property of S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate

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Technology Process of S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate

There total 5 articles about S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1403889-62-2
S-2-(acetoxy(2-fluorophenyl)amino)-2-oxoethyl O-ethyl carbonodithioate

: 72824-04-5
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1403889-71-3
S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; for 5h; Reflux; Inert atmosphere;
DOI:10.1021/ol3026044

Reference yield:

: 1403889-51-9
C₈H₇ClFNO₂

: 1403889-71-3
S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / 20 °C / Inert atmosphere

2: acetone / 6 h / Inert atmosphere

3: dilauryl peroxide / ethyl acetate / 5 h / Reflux; Inert atmosphere

With dilauryl peroxide; acetic anhydride; In ethyl acetate; acetone;
DOI:10.1021/ol3026044

Reference yield:

: N-acetoxy-N-(2-fluorophenyl)-2-chloroacetamide

: 1403889-71-3
S-5-(acetoxy(2-fluorophenyl)amino)-5-oxo-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentan-2-yl O-ethyl carbonodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 6 h / Inert atmosphere

2: dilauryl peroxide / ethyl acetate / 5 h / Reflux; Inert atmosphere

With dilauryl peroxide; In ethyl acetate; acetone;
DOI:10.1021/ol3026044