N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate

Base Information

• Chemical Name: N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate
• CAS No.: 1067583-19-0
• Molecular Formula: C₅H₁₁NO*C₉H₉N₃O₂S
• Molecular Weight: 324.404
• Mol file: 1067583-19-0.mol

Synonyms:N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate

Chemical Property of N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate

There total 1 articles about N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-methyl-morpholine (109-02-4) + cyanothioacetamide (503621-72-5) + ethyl (ethoxymethylene)cyanoacetate (42466-67-1,42466-69-3) → N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate (1067583-19-0)

Guidance literature:

In ethanol; at 20 ℃;

DOI:10.1007/s10593-007-0143-5

Reference yield: 83.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate (1067583-19-0) + ortho-phenitidine (94-70-2) → 7-cyano-3-(2-ethoxyphenyl)-6-thioxo-1,3,4,6-tetrahydro-2H-pyrido[1,2-a][1,3,5]triazine-9-carboxylic acid ethyl ether (919720-63-1)

Guidance literature:

In ethanol; Heating;

DOI:10.1007/s10593-007-0143-5

Reference yield: 81.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + N-methylmorpholinium 1-amino-2,4-dicyano-4-ethoxycarbonyl-1,3-butadienethiolate (1067583-19-0) + aniline (62-53-3) → 7-cyano-3-phenyl-6-thioxo-1,3,4,6-tetrahydro-2H-pyrido[1,2-a][1,3,5]triazine-9-carboxylic acid ethyl ether (1067583-24-7)

Guidance literature:

In ethanol; Heating;

DOI:10.1007/s10593-007-0143-5

upstream raw materials:

4-methyl-morpholine

cyanothioacetamide

ethyl (ethoxymethylene)cyanoacetate

Downstream raw materials:

7-cyano-3-(3,4-dimethylphenyl)-6-thioxo-1,3,4,6-tetrahydro-2H-pyrido[1,2-a][1,3,5]triazine-9-carboxylic acid ethyl ether

7-cyano-3-phenyl-6-thioxo-1,3,4,6-tetrahydro-2H-pyrido[1,2-a][1,3,5]triazine-9-carboxylic acid ethyl ether

7-cyano-3-(2-ethoxyphenyl)-6-thioxo-1,3,4,6-tetrahydro-2H-pyrido[1,2-a][1,3,5]triazine-9-carboxylic acid ethyl ether

7-cyano-3-(4-fluorophenyl)-6-thioxo-1,3,4,6-tetrahydro-2H-pyrido[1,2-a][1,3,5]triazine-9-carboxylic acid ethyl ether