(E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

Base Information

Chemical Name:(E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide
CAS No.:1350468-27-7
Molecular Formula:C₁₄H₂₀BrNO₂S
Molecular Weight:346.288
Hs Code.:

Synonyms:(E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

Suppliers and Price of (E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

Chemical Property:

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Technology Process of (E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

There total 10 articles about (E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: N-(2-hydroxyethyl)-4-methyl-N-((E)-2-methylbut-2-en-1-yl)benzenesulfonamide

: 1350468-27-7
(E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 16h;
DOI:10.1021/jacs.7b06794

Reference yield:

: 497-02-9
(E)-2-methyl-2-buten-1-ol

: 1350468-27-7
(E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine

2: trifluoroacetic acid

3: caesium carbonate

With di-isopropyl azodicarboxylate; caesium carbonate; triphenylphosphine; trifluoroacetic acid; 1: Mitsunobu reaction;
DOI:10.1021/ja2091883

Reference yield:

: 14316-14-4
N-(2-hydroxy-ethyl)-4-methyl-benzenesulfonamide

: 1350468-27-7
(E)-N-(2-bromoethyl)-4-methyl-N-(2-methylbut-2-en-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / 16 h / Reflux

2: triphenylphosphine; carbon tetrabromide / tetrahydrofuran / 16 h / 0 - 20 °C

With carbon tetrabromide; potassium carbonate; triphenylphosphine; potassium iodide; In tetrahydrofuran; acetone;
DOI:10.1021/jacs.7b06794