tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate

Base Information

Chemical Name:tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate
CAS No.:1190850-93-1
Molecular Formula:C₁₈H₂₇NO₅
Molecular Weight:337.416
Hs Code.:

Synonyms:tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate

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Technology Process of tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate

There total 1 articles about tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1190850-92-0
tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(trityloxymethyl)tetrahydrofuran-2-yl]methylcarbamate

: 1190850-93-1
tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; at 40 ℃; for 6h;
DOI:10.1002/ejoc.200900460

Reference yield: 80.0%

: 1190850-93-1
tert-butyl [(2R,3S,5R)-3-(benzyloxy)-5-(hydroxymethyl)tetrahydrofuran-2-yl]methylcarbamate

: 1190850-94-2
(2R,4S,5R)-4-(benzyloxy)-5-[(tert-butoxycarbonylamino)methyl]tetrahydrofuran-2-carboxylic acid

Guidance literature:: With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium chloride; potassium bromide; In acetonitrile; at 0 ℃; for 1h;
DOI:10.1002/ejoc.200900460