Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind

Base Information

Chemical Name:Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind
CAS No.:1037077-45-4
Molecular Formula:C₃₁H₃₇N₇O₄
Molecular Weight:571.679
Hs Code.:

Synonyms:Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind

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Chemical Property of Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind

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Technology Process of Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind

There total 6 articles about Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1414524-28-9
C₃₁H₂₉N₉O₅

: 108-91-8,157973-60-9
cyclohexylamine

: 1037077-45-4
Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1021/jo302238u

Reference yield:

: 120122-47-6
1-methyl-4-nitro-2-trichloroacetylpyrrole

: 1037077-45-4
Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind

Guidance literature:: Multi-step reaction with 6 steps

1.1: 0.5 h

2.1: sodium tetrahydroborate; 5%-palladium/activated carbon / methanol; ethyl acetate; water / 0 °C

3.1: benzotriazol-1-ol / N,N-dimethyl-formamide / 7 h

3.2: 24 h

4.1: lithium hydroxide monohydrate; water / 1,4-dioxane / 168 h

5.1: N,N,N',N'-tetramethylformamidium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 20 °C

With sodium tetrahydroborate; lithium hydroxide monohydrate; 5%-palladium/activated carbon; N,N,N',N'-tetramethylformamidium hexafluorophosphate; water; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jo302238u

Reference yield:

: 96-54-8
N-Methylpyrrole

: 1037077-45-4
Cycl-N-methyl-pyrrolcarboxamide-γ-aminobutyric acid-N-methyl-pyrrolcarboxamide-Ind

Guidance literature:: Multi-step reaction with 10 steps

1.1: diethyl ether

2.1: nitric acid; acetic anhydride / isopropyl alcohol / -40 °C

3.1: triethylamine / ethyl acetate / 4 h / 20 °C

4.1: sodium tetrahydroborate; 5%-palladium/activated carbon / ethyl acetate; ethanol; water / 0 - 20 °C

5.1: dmap / 7 h

5.2: DIPC / 24 h

6.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 12 h

7.1: benzotriazol-1-ol / N,N-dimethyl-formamide / 7 h

7.2: 24 h

8.1: lithium hydroxide monohydrate; water / 1,4-dioxane / 168 h

9.1: N,N,N',N'-tetramethylformamidium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

10.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 72 h / 20 °C

With dmap; sodium tetrahydroborate; lithium hydroxide monohydrate; 5%-palladium/activated carbon; N,N,N',N'-tetramethylformamidium hexafluorophosphate; water; nitric acid; acetic anhydride; benzotriazol-1-ol; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; water; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo302238u