Technology Process of C36H34O12
There total 6 articles about C36H34O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 1 h / 0 °C
1.2: 5 h / 0 - 20 °C
2.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 0.5 h / -78 °C
2.2: 2 h / -78 - -20 °C
3.1: boron trichloride / dichloromethane / 0.67 h / 20 °C
4.1: disodium hydrogenphosphate / acetonitrile / 3 h / 20 °C
5.1: silver trifluoroacetate; triethylamine / 1,2-dichloro-ethane / 20 h / 60 °C
6.1: pyridine / 0.5 h / 20 °C
With
pyridine; disodium hydrogenphosphate; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; silver trifluoroacetate; pivaloyl chloride; boron trichloride; triethylamine;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.062
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron trichloride / dichloromethane / 0.67 h / 20 °C
2: disodium hydrogenphosphate / acetonitrile / 3 h / 20 °C
3: silver trifluoroacetate; triethylamine / 1,2-dichloro-ethane / 20 h / 60 °C
4: pyridine / 0.5 h / 20 °C
With
pyridine; disodium hydrogenphosphate; silver trifluoroacetate; boron trichloride; triethylamine;
In
dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.062