C₂₈H₂₅N₃O

Base Information

• Chemical Name: C₂₈H₂₅N₃O
• CAS No.: 1384454-13-0
• Molecular Formula: C₂₈H₂₅N₃O
• Molecular Weight: 419.526
• Mol file: 1384454-13-0.mol

Synonyms:C₂₈H₂₅N₃O

Chemical Property of C₂₈H₂₅N₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₂₅N₃O

There total 4 articles about C₂₈H₂₅N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-(3-bromopropoxy)-4-(triphenylmethyl)benzene (930279-14-4) → C28H25N3O (1384454-13-0)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 50 ℃; for 5h;

DOI:10.1039/c2cc32865h

Reference yield: 73.0%

C35H32O4S → C28H25N3O (1384454-13-0)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 70 ℃; for 15h; Inert atmosphere;

DOI:10.1021/jacs.9b07143

Reference yield:

phenol (108-95-2,27073-41-2) → C28H25N3O (1384454-13-0)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogenchloride / water / 6 h / 160 °C

2: potassium carbonate / acetone / 24 h / Reflux

3: dmap; triethylamine / dichloromethane / 20 °C

4: sodium azide / N,N-dimethyl-formamide / 15 h / 70 °C / Inert atmosphere

With hydrogenchloride; dmap; sodium azide; potassium carbonate; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide; acetone;

DOI:10.1021/jacs.9b07143

upstream raw materials:

1-(3-bromopropoxy)-4-(triphenylmethyl)benzene

phenol

triphenylmethyl alcohol