Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose

Base Information

Chemical Name:Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose
CAS No.:109978-66-7
Molecular Formula:C₁₆H₂₁NO₅
Molecular Weight:307.346
Hs Code.:

Synonyms:Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose

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Chemical Property of Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose

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Technology Process of Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose

There total 2 articles about Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 3-benzyloxycarbonylamino-2,3,6-trideoxy-3-C-methyl-α,β-L-ribo-hexopyranoside

: methyl 3-benzyloxycarbonylamino-2,3,6-trideoxy-3-C-methyl-β-L-threo-hexopyranos-4-uloside

: 109978-66-7
Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose

Guidance literature:: With dipyridinium dichromate; acetic acid; In dichloromethane; at 55 ℃; for 24h; Overall yield = 90 %; Overall yield = 2 g; Inert atmosphere;
DOI:10.1021/acs.orglett.8b01355

Reference yield:

: 109978-55-4
Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-α-L-erythro-hexopyranosid-4-ulose

: 74-88-4
methyl iodide

: 109978-65-6
Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-erythro-hexopyranosid-4-ulose

: 109978-66-7
Methyl-3-<(benzyloxycarbonyl)amino>-2,3,6-tridesoxy-3-C-methyl-α-L-threo-hexopyranosid-4-ulose

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 45 min, 2.) HMPA, -78 deg C to RT in 30 min;