(2,2-Diethyl-1,3-dioxopropane-1,3-diyl)dicarbamic acid diethyl ester

Base Information

• Chemical Name: (2,2-Diethyl-1,3-dioxopropane-1,3-diyl)dicarbamic acid diethyl ester
• CAS No.: 63884-60-6
• Molecular Formula: C13H22 N2 O6
• Molecular Weight: 302.327
• Hs Code.: 2924199090

Synonyms:Malonamide,N,N'-diethoxycarbonyl-2,2-diethyl;MC 2659;

Chemical Property of (2,2-Diethyl-1,3-dioxopropane-1,3-diyl)dicarbamic acid diethyl ester

Chemical Property:

• PKA: 7.28±0.46(Predicted)
• PSA: 117.78000
• Density: 1.153g/cm³
• LogP: 3.01880

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,2-Diethyl-1,3-dioxopropane-1,3-diyl)dicarbamic acid diethyl ester

There total 2 articles about (2,2-Diethyl-1,3-dioxopropane-1,3-diyl)dicarbamic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

urethane (51-79-6) + diethylmalonyl chloride (54505-72-5) → N,N'-bis-ethoxycarbonyl-2,2-diethyl-malonic acid diamide (63884-60-6)

Guidance literature:

With xylene; durch Erhitzen bis zum Aufhoeren der Chlorwasserstoff-Entwicklung;

Reference yield:

urethane (51-79-6) + diethylmalonyl chloride (54505-72-5) → N,N'-bis-ethoxycarbonyl-2,2-diethyl-malonic acid diamide (63884-60-6) + 5,5-diethyl-2,4,6-trioxo-tetrahydro-pyrimidine-1-carboxylic acid ethyl ester (500336-55-0)

Guidance literature:

With xylene;

Reference yield:

N,N'-bis-ethoxycarbonyl-2,2-diethyl-malonic acid diamide (63884-60-6) → diethylbarbituric acid (57-44-3)

Guidance literature:

With sodium ethanolate;

upstream raw materials:

urethane

diethylmalonyl chloride

Downstream raw materials:

1,3-diethylbarbituric acid

diethylbarbituric acid

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