trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol

Base Information

Chemical Name:trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol
CAS No.:89726-86-3
Molecular Formula:C₁₅H₃₀O₃
Molecular Weight:258.401
Hs Code.:

Synonyms:trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol

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Technology Process of trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol

There total 2 articles about trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 89726-83-0,89746-17-8
trans-4-tert-butyl-O-(methoxymethyl)-1-(tri-n-butylstannyl)cyclohexanol

: 67-64-1
acetone

: 89726-86-3
trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol

Guidance literature:: With n-butyllithium; In 1,2-dimethoxyethane; at -78 ℃;
DOI:10.1021/ja00211a024

Reference yield: 70.0%

: 109-72-8,29786-93-4
n-butyllithium

: 89726-83-0,89746-17-8
trans-4-tert-butyl-O-(methoxymethyl)-1-(tri-n-butylstannyl)cyclohexanol

: 89726-86-3
trans-4-tert-butyl-1-(1-hydroxy-1-methylethyl)-O-(methoxymethyl)cyclohexanol

Guidance literature:: With acetone; In 1,2-dimethoxyethane; under argon; tin-compound in DME cooled to -78 °C; LiBu was added over 10 s; after 2 min quenched with acetone;; poured into NH4Cl-soln. and petroleum ether, shaked 1 min, organic layer sepd., washed (brine), dried (Na2SO4), filtered, concd. (vacuo); chromd. (silica gel; ethyl acetate/petroleum ether 1.5:98.5); (1)H- and (13)C-NMR; IR; MAS;;
DOI:10.1021/ja00211a024