C₂₃H₂₅F₆NO

Base Information

Chemical Name:C₂₃H₂₅F₆NO
CAS No.:1429045-48-6
Molecular Formula:C₂₃H₂₅F₆NO
Molecular Weight:445.448
Hs Code.:

C<sub>23</sub>H<sub>25</sub>F<sub>6</sub>NO

Synonyms:C₂₃H₂₅F₆NO

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Chemical Property of C₂₃H₂₅F₆NO

Chemical Property:

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Technology Process of C₂₃H₂₅F₆NO

There total 11 articles about C₂₃H₂₅F₆NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1429045-46-4
C₂₂H₂₃F₆NO

: 1429045-48-6
C₂₃H₂₅F₆NO

Guidance literature:: With formic acid; In chloroform; at 65 ℃; for 12h;
DOI:10.1016/j.bmc.2013.02.010

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 1429045-48-6
C₂₃H₂₅F₆NO

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrahydrofuran / 1 h / 0 - 20 °C

1.2: 20 °C

2.1: trimethylamine hydrochloride / water; N,N-dimethyl-formamide / 6 h / 93 °C

3.1: pyridinium p-toluenesulfonate / benzene / 111 °C / Dean-Stark

4.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

5.1: sodium tetrahydroborate / methanol / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

7.1: hydrogenchloride / water; acetone / 2 h / Reflux

8.1: sodium azide; trifluoroacetic acid / water; benzene / 1 h / 65 °C

8.2: Chiralpak AS semi-prep column / Resolution of racemate

9.1: borane-THF / 20 - 65 °C

10.1: formic acid / chloroform / 12 h / 65 °C

With hydrogenchloride; sodium tetrahydroborate; formic acid; sodium azide; borane-THF; pyridinium p-toluenesulfonate; trimethylamine hydrochloride; sodium hydride; diisobutylaluminium hydride; trifluoroacetic acid; In tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide; acetone; toluene; mineral oil; benzene; 2.1: |Michael Addition / 8.1: |Schmidt Reaction;
DOI:10.1016/j.bmc.2013.02.010

Reference yield:

: 10345-87-6
3-phenylcyclohex-2-enone

: 1429045-48-6
C₂₃H₂₅F₆NO

Guidance literature:: Multi-step reaction with 9 steps

1.1: trimethylamine hydrochloride / water; N,N-dimethyl-formamide / 6 h / 93 °C

2.1: pyridinium p-toluenesulfonate / benzene / 111 °C / Dean-Stark

3.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

4.1: sodium tetrahydroborate / methanol / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C

6.1: hydrogenchloride / water; acetone / 2 h / Reflux

7.1: sodium azide; trifluoroacetic acid / water; benzene / 1 h / 65 °C

7.2: Chiralpak AS semi-prep column / Resolution of racemate

8.1: borane-THF / 20 - 65 °C

9.1: formic acid / chloroform / 12 h / 65 °C

With hydrogenchloride; sodium tetrahydroborate; formic acid; sodium azide; borane-THF; pyridinium p-toluenesulfonate; trimethylamine hydrochloride; sodium hydride; diisobutylaluminium hydride; trifluoroacetic acid; In methanol; chloroform; water; N,N-dimethyl-formamide; acetone; toluene; mineral oil; benzene; 1.1: |Michael Addition / 7.1: |Schmidt Reaction;
DOI:10.1016/j.bmc.2013.02.010