1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone

Base Information

• Chemical Name: 1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone
• CAS No.: 87880-47-5
• Molecular Formula: C₂₀H₁₅N₃O₄
• Molecular Weight: 361.357
• Mol file: 87880-47-5.mol

Synonyms:1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone

Chemical Property of 1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone

There total 3 articles about 1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine (57492-77-0) + acetone (67-64-1) → benzamide (55-21-0,27208-38-4) + 1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone (87880-47-5) + 2-methyl-6,7-methylenedioxy-quinazoline (58277-03-5)

Guidance literature:

for 60h; Ambient temperature; Irradiation;

DOI:10.1039/P19830002003

Reference yield: 2.6%

N-<2-methyl-6,7-methylenedioxy-4-(2-oxopropylidene)-3,4-dihydroquinazolin-3-yl>benzamide (87880-49-7) → 1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone (87880-47-5)

Guidance literature:

In acetone; for 35h; Ambient temperature; Irradiation;

DOI:10.1039/P19830002003

Reference yield:

N-[6-Methyl-8-(2-oxo-propyl)-8H-[1,3]dioxolo[4,5-g]quinazolin-7-yl]-benzamide (80056-18-4) → 1-benzoylimino-1-(2-methyl-6,7-methylenedioxyquinazolin-4-yl)acetone (87880-47-5)

Guidance literature:

Multi-step reaction with 2 steps

1: oxygen / acetone / 50 h / Ambient temperature; Irradiation

2: 2.6 percent / acetone / 35 h / Ambient temperature; Irradiation

With oxygen; In acetone;

DOI:10.1039/P19830002003

upstream raw materials:

N-<2-methyl-6,7-methylenedioxy-4-(2-oxopropylidene)-3,4-dihydroquinazolin-3-yl>benzamide

7-benzoylamino-6-methyl-[1,3]dioxolo[4,5-g]quinazolinium betaine

acetone

N-[6-Methyl-8-(2-oxo-propyl)-8H-[1,3]dioxolo[4,5-g]quinazolin-7-yl]-benzamide