1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

Base Information

Chemical Name:1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione
CAS No.:187040-43-3
Molecular Formula:C₃₅H₃₂N₂O₆
Molecular Weight:576.649
Hs Code.:

Synonyms:1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

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Chemical Property of 1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

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Technology Process of 1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

There total 8 articles about 1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 187040-42-2
1-Acetyl-4-benzyl-3-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-6-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

: 187040-43-3
1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: With hydrazine hydrate; In N,N-dimethyl-formamide; for 1h; Ambient temperature;

Reference yield:

: 80592-18-3
3,4-methylenedioxyphenyl formate

: 187040-43-3
1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: Multi-step reaction with 6 steps

1: 10percent aq. KOH / methanol / 2.5 h / Ambient temperature

2: 56 percent / CF₃COOH / 4 h / Heating

3: 88 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 1 h

4: 78 percent / t-BuOK / 2-methyl-propan-2-ol; dimethylformamide / 24 h / Ambient temperature

5: 100 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) r.t., 2 h

6: 83 percent / NH₂NH₂*H₂O / dimethylformamide / 1 h / Ambient temperature

With potassium hydroxide; potassium tert-butylate; sodium hydride; hydrazine hydrate; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 533-31-3
Sesamol

: 187040-43-3
1-Benzyl-6-[1-(6-benzyloxy-benzo[1,3]dioxol-5-yl)-meth-(Z)-ylidene]-3-(4-methoxy-3-methyl-benzyl)-piperazine-2,5-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 56 percent / CF₃COOH / 4 h / Heating

2: 88 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) 0 deg C, 1 h

3: 78 percent / t-BuOK / 2-methyl-propan-2-ol; dimethylformamide / 24 h / Ambient temperature

4: 100 percent / NaH / dimethylformamide / 1.) 0 deg C, 30 min, 2.) r.t., 2 h

5: 83 percent / NH₂NH₂*H₂O / dimethylformamide / 1 h / Ambient temperature

With potassium tert-butylate; sodium hydride; hydrazine hydrate; trifluoroacetic acid; In N,N-dimethyl-formamide; tert-butyl alcohol;