3,3′-dinitrobenzhydrol

Base Information

• Chemical Name: 3,3′-dinitrobenzhydrol
• CAS No.: 51339-33-4
• Molecular Formula: C₁₃H₁₀N₂O₅
• Molecular Weight: 274.233
• Mol file: 51339-33-4.mol

Synonyms:3,3′-dinitrobenzhydrol

Chemical Property of 3,3′-dinitrobenzhydrol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3′-dinitrobenzhydrol

There total 3 articles about 3,3′-dinitrobenzhydrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3,3'-dinitrobenzophenone (21222-05-9) → 3,3′-dinitrobenzhydrol (51339-33-4)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 1h;

DOI:10.1016/S0040-4039(02)02209-8

Reference yield: 68.0%

[bis(p-anisyl)methyl] [bis(m-nitrophenyl)methyl] ether (1426391-59-4) → bis(p-methoxyphenyl)methanone (90-96-0) + 4,4'-dianisylmethane (726-18-1) + 3,3′-dinitrobenzhydrol (51339-33-4)

Guidance literature:

With iodine; In neat (no solvent); at 85 ℃; for 18h;

DOI:10.1039/c3ob27267b

Reference yield:

3,3'-dinitro-benzophenone-hydrazone (100382-66-9) → 3,3′-dinitrobenzhydrol (51339-33-4)

Guidance literature:

Multi-step reaction with 2 steps

1: HgO

2: aq. TsOH / acetonitrile

With toluene-4-sulfonic acid; mercury(II) oxide; In acetonitrile;

DOI:10.1039/jr9630003808

upstream raw materials:

3,3'-dinitrobenzophenone

3,3'-dinitro-benzophenone-hydrazone

[bis(p-anisyl)methyl] [bis(m-nitrophenyl)methyl] ether

Downstream raw materials:

β-m-Nitrophenyl-m-nitro-hydrozimtsaeure

3,3-bis(3-nitrophenyl)acrylic acid

3,3'-Dinitro-benzhydrylbromid

1-fluoro-bis[1-(3-nitrophenyl)]methane