o-Methylbenzophenon-O-methyloxim

Base Information

• Chemical Name: o-Methylbenzophenon-O-methyloxim
• CAS No.: 71104-34-2
• Molecular Formula: C₁₅H₁₅NO
• Molecular Weight: 225.29
• Mol file: 71104-34-2.mol

Synonyms:o-Methylbenzophenon-O-methyloxim

Chemical Property of o-Methylbenzophenon-O-methyloxim

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of o-Methylbenzophenon-O-methyloxim

There total 1 articles about o-Methylbenzophenon-O-methyloxim which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

C8H8BrNO (344326-00-7) + 2-Methylphenylboronic acid (16419-60-6) → o-Methylbenzophenon-O-methyloxim (71104-34-2)

Guidance literature:

With palladium diacetate; caesium carbonate; triphenylphosphine; In toluene; for 3h; Reflux;

DOI:10.1248/cpb.59.1206

Reference yield: 88.0%

o-Methylbenzophenon-O-methyloxim (71104-34-2) → C15H15NO2

Guidance literature:

With Oxone; palladium diacetate; triphenylphosphine; In 1,1,2,2-tetrachloroethane; at 80 ℃; for 24h;

DOI:10.1021/acscatal.5b01700

Reference yield: 63.0%

o-Methylbenzophenon-O-methyloxim (71104-34-2) → C15H14N2O3

Guidance literature:

With tert.-butylnitrite; tetrabutylammomium bromide; oxygen; palladium diacetate; In chlorobenzene; at 80 ℃; for 24h; under 760.051 Torr; regioselective reaction;

DOI:10.1021/cs502126n

upstream raw materials:

C₈H₈BrNO

2-Methylphenylboronic acid