1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole

Base Information

• Chemical Name: 1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole
• CAS No.: 149202-71-1
• Molecular Formula: C₁₃H₁₉N₅O
• Molecular Weight: 261.327
• Mol file: 149202-71-1.mol

Synonyms:1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole

Chemical Property of 1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole

There total 1 articles about 1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-[5-Methyl-3-(2-nitro-phenyl)-4,5-dihydro-3H-[1,2,3]triazol-4-yl]-morpholine → 1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole (149202-71-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;

Reference yield: 92.0%

1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole (149202-71-1) → 2-methylquinoxaline (7251-61-8)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; Mechanism; multistep reaction thermal rearrangement of other 1,2,3-triazoles;

Reference yield: 12.0%

1-(2-Aminophenyl)-4,5-dihydro-4-methyl-5-morpholino-1,2,3-triazole (149202-71-1) → 2-methylquinoxaline (7251-61-8) + 2-ethylbenzimidazole (1848-84-6) + 2-methyl-1,2,3,4-tetrahydroquinoxaline (6640-55-7,24463-30-7,24463-31-8,49849-47-0)

Guidance literature:

palladium on activated charcoal; Yield given. Multistep reaction; 1) toluene, reflux, 1h, 2) ethanol, reflux, 30 min;

Downstream raw materials:

2-methylquinoxaline

2-ethylbenzimidazole

2-methyl-1,2,3,4-tetrahydroquinoxaline