C₃₀H₄₉BO₆

Base Information

Chemical Name:C₃₀H₄₉BO₆
CAS No.:1330569-48-6
Molecular Formula:C₃₀H₄₉BO₆
Molecular Weight:516.526
Hs Code.:

C<sub>30</sub>H<sub>49</sub>BO<sub>6</sub>

Synonyms:C₃₀H₄₉BO₆

Suppliers and Price of C₃₀H₄₉BO₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₀H₄₉BO₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₀H₄₉BO₆

There total 1 articles about C₃₀H₄₉BO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: (4S,5S,6S,7E)-2-bromo-6-ethyl-8-(4-methoxybenzyloxy)methyl-5-methoxymethoxy-4-methyldeca-2,7-diene

: 73183-34-3
bis(pinacol)diborane

: 1330569-48-6
C₃₀H₄₉BO₆

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium phenolate; triphenylphosphine; In toluene; at 50 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.006

Reference yield:

: 1330569-48-6
C₃₀H₄₉BO₆

: 1330569-60-2
C₃₀H₄₀O₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.67 h / 0 - 20 °C / aq. phosphate buffer

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 2,6-di-tert-butyl-4-methyl-phenol; sodium hydroxide / tetrahydrofuran; water / 20 h / 20 °C / Inert atmosphere

3.1: 2,6-di-tert-butyl-4-methyl-phenol; sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.25 h / 0 - 20 °C

4.1: 2,6-di-tert-butyl-4-methyl-phenol / toluene / 21 h / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.5 h / 0 - 20 °C

5.2: 0 °C / Saturated solution

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 10.5 h / Reflux

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

7.2: 0 °C / Saturated solution

8.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

9.2: 3 h / -78 - 0 °C / Inert atmosphere

10.1: camphor-10-sulfonic acid / methanol / 120 h / 40 °C

11.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; n-butyllithium; 2,6-di-tert-butyl-4-methyl-phenol; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene; 2.1: Suzuki-Miyaura coupling / 3.1: Dess-Martin oxidation / 8.1: Dess-Martin oxidation / 9.2: Horner-Wadsworth-Emmons olefination / 11.1: Dess-Martin oxidation;
DOI:10.1016/j.tet.2011.04.006

Reference yield:

: 1330569-48-6
C₃₀H₄₉BO₆

: (+)-zyggomphic acid

Guidance literature:: Multi-step reaction with 12 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.67 h / 0 - 20 °C / aq. phosphate buffer

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 2,6-di-tert-butyl-4-methyl-phenol; sodium hydroxide / tetrahydrofuran; water / 20 h / 20 °C / Inert atmosphere

3.1: 2,6-di-tert-butyl-4-methyl-phenol; sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.25 h / 0 - 20 °C

4.1: 2,6-di-tert-butyl-4-methyl-phenol / toluene / 21 h / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.5 h / 0 - 20 °C

5.2: 0 °C / Saturated solution

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 10.5 h / Reflux

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

7.2: 0 °C / Saturated solution

8.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

9.2: 3 h / -78 - 0 °C / Inert atmosphere

10.1: camphor-10-sulfonic acid / methanol / 120 h / 40 °C

11.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

12.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 6 h / 0 - 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; 2,6-di-tert-butyl-4-methyl-phenol; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene; tert-butyl alcohol; 2.1: Suzuki-Miyaura coupling / 3.1: Dess-Martin oxidation / 8.1: Dess-Martin oxidation / 9.2: Horner-Wadsworth-Emmons olefination / 11.1: Dess-Martin oxidation / 12.1: Kraus-Pinnick oxidation;
DOI:10.1016/j.tet.2011.04.006