Technology Process of C11H10ClN3OS
There total 6 articles about C11H10ClN3OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; acetic acid;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: magnesium(II) chloride hexahydrate; sodium monohydrogen sulfide x-hydrate / N,N-dimethyl-formamide / 2 h / 20 °C
2.1: diethyl ether / 24 h
3.1: N,N-dimethyl-formamide / 90 °C / Inert atmosphere
4.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C
4.2: 12 h / 125 °C
5.1: N,N,N,N,N,N-hexamethylphosphoric triamide / 20 °C
6.1: dihydrogen peroxide; acetic acid / 20 °C
With
sodium monohydrogen sulfide x-hydrate; magnesium(II) chloride hexahydrate; dihydrogen peroxide; sodium hydride; acetic acid;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diethyl ether / 24 h
2.1: N,N-dimethyl-formamide / 90 °C / Inert atmosphere
3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C
3.2: 12 h / 125 °C
4.1: N,N,N,N,N,N-hexamethylphosphoric triamide / 20 °C
5.1: dihydrogen peroxide; acetic acid / 20 °C
With
dihydrogen peroxide; sodium hydride; acetic acid;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N,N-dimethyl-formamide;