Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

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Chemical Name:Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester
CAS No.:193285-11-9
Molecular Formula:C₁₆H₂₆NO₉P
Molecular Weight:407.357
Hs Code.:

Synonyms:Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

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Chemical Property of Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

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Technology Process of Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

There total 3 articles about Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.9%

: 193285-10-8
D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

: 193285-11-9
Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: With trifluoroacetic acid; In water; at 20 ℃; for 0.25h;
DOI:10.1016/S0008-6215(97)00109-2

Reference yield:

: 54750-12-8
(2R,4S,5R)-2-chloro-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidin-2-one

: 193285-11-9
Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1) DMF, 0 deg C, 1 h; 2) DMF, 2 h, 0 deg C

2: 97.9 percent / CF₃COOH / H₂O / 0.25 h / 20 °C

With sodium hydride; trifluoroacetic acid; In water;
DOI:10.1016/S0008-6215(97)00109-2

Reference yield:

: 34361-60-9,55123-24-5,55123-26-7,62012-78-6,104873-71-4
1,2:4,5-dicyclohexylidene-myo-inositol

: 193285-11-9
Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1) DMF, 0 deg C, 1 h; 2) DMF, 2 h, 0 deg C

2: 97.9 percent / CF₃COOH / H₂O / 0.25 h / 20 °C

With sodium hydride; trifluoroacetic acid; In water;
DOI:10.1016/S0008-6215(97)00109-2