D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

Base Information

Chemical Name:D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol
CAS No.:193285-10-8
Molecular Formula:C₂₈H₄₀NO₈P
Molecular Weight:549.601
Hs Code.:

Synonyms:D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

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Technology Process of D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

There total 1 articles about D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54750-12-8
(2R,4S,5R)-2-chloro-3,4-dimethyl-5-phenyl-1,3,2-oxazaphospholidin-2-one

: 34361-60-9,55123-24-5,55123-26-7,62012-78-6,104873-71-4
1,2:4,5-dicyclohexylidene-myo-inositol

: 193285-10-8
D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

: C₂₈H₄₀NO₈P

Guidance literature:: With sodium hydride; Yield given. Multistep reaction. Yields of byproduct given; 1) DMF, 0 deg C, 1 h; 2) DMF, 2 h, 0 deg C;
DOI:10.1016/S0008-6215(97)00109-2

Reference yield: 97.9%

: 193285-10-8
D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

: 193285-11-9
Phosphoric acid (1R,2S)-2-methylamino-1-phenyl-propyl ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl ester

Guidance literature:: With trifluoroacetic acid; In water; at 20 ℃; for 0.25h;
DOI:10.1016/S0008-6215(97)00109-2

Reference yield:

: 193285-10-8
D-1,2;4,5-di-O-cyclohexylidene-3-((2'S,4'S,5'R)-3',4'-dimethyl-5'-phenyl-1',3',2'-oxazaphospholidin-2'-one)-myo-inositol

: 14980-89-3,15065-15-3,16006-20-5,32739-43-8,37170-04-0,53797-24-3,70470-66-5,103529-92-6,106032-58-0,106032-59-1,106707-92-0,111956-21-9,114884-35-4,125356-28-7,126722-33-6
D-myo-inositol-3-phosphate biscyclohexylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1: 97.9 percent / CF₃COOH / H₂O / 0.25 h / 20 °C

2: H₂ / palldium on carbon / methanol; H₂O / 16 h / 20 °C / 2585.7 Torr

3: H₂O / 4 h / 20 °C

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In methanol; water;
DOI:10.1016/S0008-6215(97)00109-2