5-phenyl)methyl>-1H-tetrazole

Base Information

Chemical Name:5-phenyl)methyl>-1H-tetrazole
CAS No.:156575-04-1
Molecular Formula:C₁₉H₂₀N₆O
Molecular Weight:348.407
Hs Code.:

5-<amino(2-<2-(4,4-dimethyloxazolin-2-yl)phenyl>phenyl)methyl>-1H-tetrazole

Synonyms:5-phenyl)methyl>-1H-tetrazole

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Chemical Property of 5-phenyl)methyl>-1H-tetrazole

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Technology Process of 5-phenyl)methyl>-1H-tetrazole

There total 5 articles about 5-phenyl)methyl>-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 156574-98-0
5-cyano-7-(<2-methyl-3-hydroxy-prop-2-yl>amino)-5H-dibenzazepine

: 156575-04-1
5-phenyl)methyl>-1H-tetrazole

Guidance literature:: With tributyltin azide; at 90 ℃; for 48h;
DOI:10.1080/00397919408010202

Reference yield:

: 57598-33-1
2-(2-methoxyphenyl)-4,4-dimethyl-2-oxazoline

: 156575-04-1
5-phenyl)methyl>-1H-tetrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg / 1.) THF, reflux, 20 min, 2.) THF, RT, 16 h

2: 59 percent / aq. HCl / 2 h / Ambient temperature

3: 1.) NH₄Cl, Al₂O₃ / 1.) acetonitrile, ultrasonification, 1 h, 2.) acetonitrile, ultrasonification, overnight

4: 76 percent / tributyltin azide / 48 h / 90 °C

With hydrogenchloride; aluminum oxide; tributyltin azide; ammonium chloride; magnesium;
DOI:10.1080/00397919408010202

Reference yield:

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 156575-04-1
5-phenyl)methyl>-1H-tetrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg / 1.) THF, reflux, 20 min, 2.) THF, RT, 16 h

2: 59 percent / aq. HCl / 2 h / Ambient temperature

3: 1.) NH₄Cl, Al₂O₃ / 1.) acetonitrile, ultrasonification, 1 h, 2.) acetonitrile, ultrasonification, overnight

4: 76 percent / tributyltin azide / 48 h / 90 °C

With hydrogenchloride; aluminum oxide; tributyltin azide; ammonium chloride; magnesium;
DOI:10.1080/00397919408010202