C₃₀H₄₅N₃O₅

Base Information

• Chemical Name: C₃₀H₄₅N₃O₅
• CAS No.: 1370531-77-3
• Molecular Formula: C₃₀H₄₅N₃O₅
• Molecular Weight: 527.704
• Mol file: 1370531-77-3.mol

Synonyms:C₃₀H₄₅N₃O₅

Chemical Property of C₃₀H₄₅N₃O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₅N₃O₅

There total 8 articles about C₃₀H₄₅N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-cyclohexylmethyl-2-oxo-1,2,5,6,7,8,9,10-octahydro-cycloocta[b]pyridine-3-carboxylic acid → C30H45N3O5 (1370531-77-3)

Guidance literature:

Multi-step reaction with 5 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran

2: triethylamine / tetrahydrofuran

3: water; sodium hydroxide / tetrahydrofuran

4: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran

5: triethylamine

With oxalyl dichloride; water; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2012.02.054

Reference yield:

cyclohexylmethylamine (3218-02-8) → C30H45N3O5 (1370531-77-3)

Guidance literature:

Multi-step reaction with 8 steps

1: toluene / Reflux

2: toluene / Reflux

3: water; sodium hydroxide / tetrahydrofuran

4: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran

5: triethylamine / tetrahydrofuran

6: water; sodium hydroxide / tetrahydrofuran

7: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran

8: triethylamine

With oxalyl dichloride; water; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; toluene;

DOI:10.1016/j.bmcl.2012.02.054

Reference yield:

methyl 2-[(1-cyclohexylmethyl-2-oxo-1,2,5,6,7,8,9,10-octahydro-cycloocta[b]pyridine-3-carbonyl)-amino]-2-methyl-propionate → C30H45N3O5 (1370531-77-3)

Guidance literature:

Multi-step reaction with 3 steps

1: water; sodium hydroxide / tetrahydrofuran

2: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran

3: triethylamine

With oxalyl dichloride; water; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2012.02.054

upstream raw materials:

isonipecotic acid methyl ester

cycloactanone

C₂₁H₃₁NO₃

N-cyclohexyl-N-cyclooctylidenamine