3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one

Base Information

Chemical Name:3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one
CAS No.:944055-59-8
Molecular Formula:C₂₅H₁₇ClN₂O₄
Molecular Weight:444.874
Hs Code.:

Synonyms:3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one

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Chemical Property of 3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one

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Technology Process of 3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one

There total 2 articles about 3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 944055-46-3
3-[acetoxy(4-chlorophenyl)methyl]-4H-chromen-4-one

: 3484-10-4
2-methyl-4-nitro-1H-indole

: 944055-59-8
3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; for 1h; Heating;
DOI:10.1021/ol070878w

Reference yield:

: C₁₆H₁₁O₃Cl

: 944055-59-8
3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 1 h

2: 90 percent / AgOTf / CH₂Cl₂ / 1 h / Heating

With pyridine; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/ol070878w

Reference yield: 93.0%

: 944055-59-8
3-[(2-methyl-4-nitroindol-3-yl)-p-chlorophenylmethyl]-4H-chromen-4-one

: 2-methyl-3-(p-chlorophenyl)-4-(2-hydroxybenzoyl)-3,6-dihydro-1H-azepino[4,3,2-cd]-indole

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 2h; atmospheric pressure;
DOI:10.1021/ol070878w