bis(3-trifluoromethylphenyl)benzylphosphine oxide

Base Information

• Chemical Name: bis(3-trifluoromethylphenyl)benzylphosphine oxide
• CAS No.: 54441-77-9
• Molecular Formula: C₂₁H₁₅F₆OP
• Molecular Weight: 428.314
• Mol file: 54441-77-9.mol

Synonyms:bis(3-trifluoromethylphenyl)benzylphosphine oxide

Chemical Property of bis(3-trifluoromethylphenyl)benzylphosphine oxide

Chemical Property:

Purity/Quality:

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Technology Process of bis(3-trifluoromethylphenyl)benzylphosphine oxide

There total 2 articles about bis(3-trifluoromethylphenyl)benzylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

benzyl bromide (100-39-0) + C14H8F6OP(1-)*Li(1+) → bis(3-trifluoromethylphenyl)benzylphosphine oxide (54441-77-9)

Guidance literature:

In tetrahydrofuran; Ambient temperature;

DOI:10.1002/hlca.19830660607

Reference yield:

→ bis(3-trifluoromethylphenyl)benzylphosphine oxide (54441-77-9)

Guidance literature:

Aus m-Brombenzotrifluorid u. Diaethylphosphit;

DOI:10.1007/BF00922119

Reference yield: 91.0%

bis(3-trifluoromethylphenyl)benzylphosphine oxide (54441-77-9) → bis(3-trifluoromethylphenyl)benzylphosphine

Guidance literature:

With trichlorosilane; In triethylamine; acetonitrile; at 70 ℃; for 3h;

DOI:10.1002/hlca.19830660607

upstream raw materials:

benzyl bromide