2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide

Base Information

Chemical Name:2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide
CAS No.:88131-77-5
Molecular Formula:C₃₈H₅₁NO₂
Molecular Weight:553.828
Hs Code.:

Synonyms:2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide

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Chemical Property of 2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide

Chemical Property:

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Technology Process of 2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide

There total 3 articles about 2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 119-61-9
benzophenone

: 79288-68-9
4-tert-butyl-2,4,6-triisopropylbenzopiperidide

: 88131-77-5
2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium;
DOI:10.1021/ja00316a033

Reference yield:

: 57199-00-5
2,4,6-triisopropylbenzoyl chloride

: 88131-77-5
2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: 50 percent / TMEDA, sec-BuLi

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether;
DOI:10.1021/ja00316a033

Reference yield:

: 49623-71-4
2,4,6-triisopropylbenzoic acid

: 88131-77-5
2-(diphenylhydroxymethyl)-4-tert-butyl-2,4,6-triisopropylbenzopiperidide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 12 h / Heating

2: diethyl ether

3: 50 percent / TMEDA, sec-BuLi

With thionyl chloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether;
DOI:10.1021/ja00316a033