(S_S,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide

Base Information

• Chemical Name: (S_S,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide
• CAS No.: 902119-96-4
• Molecular Formula: C₁₆H₂₅NO₄S
• Molecular Weight: 327.445

Synonyms:(S_S,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide

Chemical Property of (S_S,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S_S,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide

There total 3 articles about (S_S,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-(3',4',5'-trimethoxyphenyl)propanal (121667-78-5) + (S)-2-methylpropane-2-sulfinamide (343338-28-3) → (SS,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide (902119-96-4)

Guidance literature:

With pyridinium p-toluenesulfonate; magnesium sulfate; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1039/b603857c

Reference yield:

3-(3,4,5-trimethoxyphenyl)propanoic acid (25173-72-2) → (SS,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide (902119-96-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 98 percent / BH₃*THF / tetrahydrofuran / 21 h / 20 °C

2: 90 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

3: 90 percent / pyridinium p-toluenesulfonate; MgSO₄ / CH₂Cl₂ / 24 h / 20 °C

With borane-THF; pyridinium p-toluenesulfonate; magnesium sulfate; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;

DOI:10.1039/b603857c

Reference yield:

3-(3,4,5-trimethoxyphenyl)propan-1-ol (53560-26-2) → (SS,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide (902119-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

2: 90 percent / pyridinium p-toluenesulfonate; MgSO₄ / CH₂Cl₂ / 24 h / 20 °C

With pyridinium p-toluenesulfonate; magnesium sulfate; Dess-Martin periodane; In dichloromethane;

DOI:10.1039/b603857c

upstream raw materials:

3-(3',4',5'-trimethoxyphenyl)propanal

(S)-2-methylpropane-2-sulfinamide

3-(3,4,5-trimethoxyphenyl)propanoic acid

3-(3,4,5-trimethoxyphenyl)propan-1-ol

Downstream raw materials:

(S_S)-N-[(S)-1-[3-(tert-butyldimethylsilyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propyl]-2-methylpropane-2-sulfinamide

(S)-(-)-N-[1-[3-(tert-butyldimethylsilyloxy)phenyl]-3-(3,4,5-trimethoxyphenyl)propyl]acetamide

C₂₀H₂₅NO₅

acetic acid (S)-(-)-3-[1-acetylamino-3-(3,4,5-trimethoxyphenyl)propyl]phenyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 902119-96-4 (S_S,E)-(+)-2-methyl-N-[3-(3,4,5-trimethoxyphenyl)propylidene]propane-2-sulfinamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send