C₃₉H₅₁Cl₂N₅O₈Si

Base Information

Chemical Name:C₃₉H₅₁Cl₂N₅O₈Si
CAS No.:1438408-37-7
Molecular Formula:C₃₉H₅₁Cl₂N₅O₈Si
Molecular Weight:816.854
Hs Code.:

C<sub>39</sub>H<sub>51</sub>Cl<sub>2</sub>N<sub>5</sub>O<sub>8</sub>Si

Synonyms:C₃₉H₅₁Cl₂N₅O₈Si

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Chemical Property of C₃₉H₅₁Cl₂N₅O₈Si

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Technology Process of C₃₉H₅₁Cl₂N₅O₈Si

There total 15 articles about C₃₉H₅₁Cl₂N₅O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1438408-36-6
C₆₀H₆₃Cl₂N₅O₁₁Si

: 1438408-37-7
C₃₉H₅₁Cl₂N₅O₈Si

Guidance literature:: C₆₀H₆₃Cl₂N₅O₁₁Si; With potassium carbonate; In methanol; at 0 ℃; for 3h; Inert atmosphere;

With water; ammonium chloride; In methanol; Inert atmosphere;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-16-2
C₁₄H₂₅NO₄

: 1438408-37-7
C₃₉H₅₁Cl₂N₅O₈Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere

2.2: 8 h / 20 °C / Inert atmosphere

2.3: 3.33 h / 20 °C / Inert atmosphere

3.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

5.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

8.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

9.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

9.2: 3 h / 50 °C / Inert atmosphere

10.1: hydrogenchloride / methanol; water / 10 h / 40 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine / 0 °C / Inert atmosphere

11.2: 0 - 20 °C / Inert atmosphere

12.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

13.1: 2,6-dimethylpyridine / dichloromethane / 6 h / -78 °C / Cooling with ice; Inert atmosphere

14.1: potassium carbonate / methanol / 3 h / 0 °C / Inert atmosphere

14.2: Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; iodine; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 4.1: |Dess-Martin Oxidation / 5.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d

Reference yield:

: 1438408-19-5
C₂₅H₃₈N₂O₇

: 1438408-37-7
C₃₉H₅₁Cl₂N₅O₈Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: C₁₅H₂₆Cl₂CuN₂O₂; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 5 h / Cooling with ice; Inert atmosphere

3.1: dichloromethane / 15 h / 50 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; mercuric triflate / dichloromethane / 10.5 h / -20 °C / Inert atmosphere; Cooling with ice

4.2: 0.5 h / -78 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / -78 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 10.33 h / -40 - -20 °C / Inert atmosphere

7.1: Trimethyl borate / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere

7.2: 3 h / 50 °C / Inert atmosphere

8.1: hydrogenchloride / methanol; water / 10 h / 40 °C / Inert atmosphere

9.1: N-ethyl-N,N-diisopropylamine / 0 °C / Inert atmosphere

9.2: 0 - 20 °C / Inert atmosphere

10.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

11.1: 2,6-dimethylpyridine / dichloromethane / 6 h / -78 °C / Cooling with ice; Inert atmosphere

12.1: potassium carbonate / methanol / 3 h / 0 °C / Inert atmosphere

12.2: Inert atmosphere

With 2,6-dimethylpyridine; hydrogenchloride; Trimethyl borate; C₁₅H₂₆Cl₂CuN₂O₂; mercuric triflate; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2.1: |Dess-Martin Oxidation / 3.1: |Wittig Olefination;
DOI:10.1039/c3cc42365d