N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

Base Information

Chemical Name:N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine
CAS No.:4512-43-0
Molecular Formula:C₂₈H₄₃N₅O₈
Molecular Weight:577.678
Hs Code.:

Synonyms:N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

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Chemical Property of N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

Chemical Property:

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Technology Process of N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

There total 11 articles about N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1312775-20-4
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

: 4512-43-0
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; at 60 ℃; for 1h;
DOI:10.1002/hlca.201400359

Reference yield:

: 15030-72-5
Z-Aib-OH

: 4512-43-0
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

Guidance literature:: Multi-step reaction with 8 steps

1: diethyl ether / 0 - 20 °C

2: hydrogenchloride; water / tetrahydrofuran / 20 °C

3: tetrahydrofuran / 4.16 h / 0 - 20 °C

4: hydrogenchloride; water / tetrahydrofuran / 2 h / 20 °C

5: N,N-dimethyl-formamide / 4.16 h / 0 - 20 °C

6: hydrogenchloride; water / tetrahydrofuran / 2.5 h / 20 °C

7: N,N-dimethyl-formamide / 0 - 20 °C

8: hydrogenchloride; water / tetrahydrofuran / 1.5 h / 60 °C

With hydrogenchloride; water; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100116

Reference yield:

: 79775-03-4
2-<2-(Benzyloxycarboxamido)-2-methylpropionamido>-2-methylpropionsaeure

: 4512-43-0
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 4.16 h / 0 - 20 °C

2: hydrogenchloride; water / tetrahydrofuran / 2 h / 20 °C

3: N,N-dimethyl-formamide / 4.16 h / 0 - 20 °C

4: hydrogenchloride; water / tetrahydrofuran / 2.5 h / 20 °C

5: N,N-dimethyl-formamide / 0 - 20 °C

6: hydrogenchloride; water / tetrahydrofuran / 1.5 h / 60 °C

With hydrogenchloride; water; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100116